WKT-C9 Automatic Karl Fischer Volumetric Titrators - Just Measure it

WKT-C9 Automatic Karl Fischer Volumetric Titrators

The WKT-C9 is a high-precision, automated Karl Fischer titrator for determining water content in solids, liquids, and powders. It’s applicable in industries such as chemicals, pharmaceuticals, petroleum, food, plastics, and more. The machine is designed to determine moisture levels as low as 10 ppm within 30 seconds and can store up to 200 sets of data.

Applications:

  • Liquids: Used in industries like chemicals (e.g., alcohols, organic solvents).
  • Solids: Ideal for the petroleum industry (e.g., insulating and transformer oils).
  • Insoluble Solids: Suitable for industries handling lithium batteries, ceramics, plastics, etc.
Technical ParameterSpecification
Product NumberWKT-C9
Measuring PrincipleKarl Fischer Volumetric Method (Permanent Stop Titration)
Minimum Titration1 μL (with 20 mL burette); 0.5 μL (optional 10 mL burette)
Measuring Range10 ppm – 100%
Moisture Range10 μg – 550 mg H₂O
Measuring Resolution1 ppm
Polarized Current±1000 μA
Burette Capacity20 mL
Burette Accuracy5E-5 (1/20,000 mL)
Titration Linear Correlation Coefficient≥ 0.999
Custom Measurement MethodsUp to 10 groups
Display and Operation4.3-inch large LCD display, key input
Stirring SpeedAdjustable
Drift Value DeductionCapable of measuring drift and customizable deduction
Special Functions– Split mixing table
– Titration delay
– End point determination delay
– Automatic cleaning
– Constant temperature stirring (optional)
Number SettingCustomizable operator and sample number
Automatic Cleaning FunctionsStartup, shutdown, pipeline, and titration pool cleaning
Data StorageUp to 200 sets
Print FunctionOptional external printer
Data CommunicationRS232 serial port for peripheral devices
Calendar/Time DisplayGLP-compliant display and printout of current time and date
End Point IndicationScreen prompt, audible warning, end light indication, and printout (requires printer)
Operating EnvironmentTemperature: 2°C – 50°C; Humidity: <90%
Power Consumption≤50 W
Host Size350 mm × 300 mm × 170 mm
Voltage220V, 50 Hz, 150 W
Weight12 KG

Instrument Characteristics:

  1. Automatic Monitoring:
    The instrument automatically adjusts itself when the measurement conditions are not met, reducing the need for extensive training for the operator.

  2. Electromagnetic Three-Way Valve:

    • Imported from Japan, this valve has a dead volume that is only 1/10th of similar domestic products.
    • It provides silent switching with a speed of 0.01 seconds, improving efficiency.
    • It can withstand up to 100 kPa of pressure, preventing leakage even if pipelines are blocked.
  3. High-Efficiency Pipeline:
    The enhanced pipeline design improves liquid filling, draining, and changing speeds, which ensures high test efficiency.

  4. Large-Screen Display and Button-Type Operation:

    • The display provides real-time feedback of current changes, making it easy to track the measurement process.
    • Quick settings and one-button operation simplify usage.
  5. Drift Measurement:
    The instrument can measure drift values and decide whether to deduct them, which is essential in harsh environments or special conditions to ensure accuracy.

  6. Custom Measurement Settings:
    It allows up to 10 different measurement method settings, accommodating various titration speeds and delay times to meet the requirements of different samples.

  7. One-Button Cleaning:
    The instrument supports several automated cleaning functions, including startup cleaning, shutdown cleaning, pipeline cleaning, and titration pool cleaning.

  8. Automatic Functions:

    • Automatic solvent absorption.
    • Automatic blanking.
    • Automatic reagent suction.
    • Automatic titration and waste discharge.
    • Automatic liquid return and cleaning.
  9. Fully Sealed Titration Cell:

    • The cell is made from corrosion-resistant PTFE material with a high borosilicate glass upper cover.
    • It minimizes environmental interference and ensures the safety of operators.
  10. Super-Large Capacity Dry Filter:
    The dry filter effectively removes environmental moisture, and consumable parts are easy to replace, enhancing operational efficiency.

  11. Noise Reduction:
    The instrument is designed to be silent during operation, which improves the working environment.

  12. RS232 Serial Port:
    This allows connection to peripheral equipment such as printers, electronic balances, and computer communication for data management and integration.

  13. Durability:

    • Made with imported materials and parts, the instrument is designed for long service life and stable performance.
    • The electrostatic spray process used in its manufacturing makes the instrument corrosion-resistant and easy to clean.
  14. Safety Features:
    The titration process occurs under solvent levels with an anti-backup device, ensuring stable titration without contamination risks.

Applicable Standards:

The WKT-C9 complies with multiple international and industry standards, including:

  • ASTM D4928-00: Standard test methods for water in crude oils by coulometric Karl Fischer titration.
  • ASTM D6304-2007: Test method for determination of water in petroleum products, lubricating oils, and additives.
  • ISO 10337-1997: Crude petroleum – determination of water using coulometric Karl Fischer titration.

Reagent Debugging and Sample Determination Steps:

  1. Reagent Debugging:

    • Connect the instrument and power it on.
    • Use methanol or another solvent to fill the electrodes.
    • Perform a blank operation to remove excess water.
    • Calibrate the Karl Fischer reagent multiple times (recommendation: use deionized water or a standard for calibration).
  2. Sample Determination:

    • Weigh the sample using an analytical balance.
    • Inject the sample into the titration cell and input the sample weight.
    • Begin the titration, and the instrument will automatically display and store the results.

Unique Features:

  • Automatic adjustments for drift values.
  • Real-time current monitoring and feedback.
  • Extensive data storage and GLP-compliant output options.
  • Advanced automation features like solvent absorption and waste discharge.

Standards Compliance:
The WKT-C9 complies with international standards such as ASTM and ISO, making it suitable for scientific and industrial use globally.

Standards Compliance:
The WKT-C9 complies with international standards such as ASTM and ISO, making it suitable for scientific and industrial use globally.

Certifications:
The product is certified under several quality management and high-tech innovation standards, ensuring its reliability and precision.

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